The Zysman-Colman Group

Important Announcements

Class hours: Mondays from 14h30 to 16h20 – course
Intensive courses: Friday January 18, 25 from 13h30-17h00
Lab hours: Thursdays from 8h30 to 17h20 – lab (group 1 - chemistry); Friday from 8h30 to 17h20 – lab (group 2 - biochemistry)
Course: D7-3021; Lab: D1-3013-3016

First course: January 14; First lab: the week of January 28
Final exam: D7-2007 (14 students) D7-3021 (60 students); Tuesday, April 16, 9h00-12h00

Course Outline

The Experiments

Course Notes

Important information and tables

pH and pKa

Thin Layer Chromatography

Following a reaction

Recrystallization and melting point

Distillation

Gas-phase chromatography

Acid/Base extraction

Liquid liquid extraction

Column Chromatography

Notes for experiment 2

Notes for experiment 3

Notes for experiment 4

Notes for experiment 5

Notes for experiment 6

Other Documents

IR software - GRAMS 32

Example of a lab notebook

Experiment 1 - ¹H NMR spectrum of the final product - MNova file; MestreC file	FTIR spectrumof the final product - Grams32 file
Experiment 2 - ¹H NMR spectrum of the final product - MNova file; MestreC file	FTIR spectrum of the final product - Grams32 file
Experiment 3 - ¹H NMR spectrum of 2-chloro-2-methylbutane - MNova file; MestreC file	FTIR spectrum of 2-chloro-2-methylbutane - Grams32 file
Experiment 3 - ¹H NMR spectrum of 2-methyl-1-butene - MNova file; MestreC file	FTIR spectrum of 2-methyl-1-butene - Grams32 file
Experiment 3 - ¹H NMR spectrum of 2-methyl-2-butene - MNova file; MestreC file	FTIR spectrum of 2-methyl-2-butene - Grams32 file
Experiment 3 - ¹H NMR spectrum of the product mixture from part 2 - MNova file; MestreC file; PDF file
Experiment 4 - ¹H NMR spectrum of florenone - MNova file; MestreC fileC	FTIR spectrum of florenone - Grams32 file
Experiment 4 - ¹H NMR spectrum of 4-methoxybenzyl alcohol - MNova file; MestreC file	FTIR spectrum of 4-methoxybenzyl alcohol - Grams32 file2
Experiment 4 - ¹H NMR spectrum of ethyl 4-aminobenzoate - MNova file; MestreC file	FTIR spectrum of ethyl 4-aminobenzoate - Grams32 file
Experiment 4 - ¹H NMR spectrum of 2-chlorobenzoic acid - MNova file; MestreC file	FTIR spectrum of 2-chlorobenzoic acid - Grams32 file
Experiment 5 - ¹H NMR spectrum of methyl 2,4-dimethylbenzoate - MNova file; MestreC file	FTIR spectrum of methyl 2,4-dimethylbenzoate - Grams32 file
Experiment 5 - ¹H NMR spectrum of methyl 3-methylbenzoate - MNova file; MestreC file	FTIR spectrum of methyl 3-methylbenzoate - Grams32 file
Experiment 6 - ¹H NMR spectrum of final product - MNova file; MestreC file	FTIR spectrum of final product - Grams32 file

Final Exmans

Final Exam (2011)	Final Exam [corrected] (2011)
Final Exam (2009)	Final Exam [corrected] (2009)
Final Exam (2008)	Final Exam [corrected] (2008)
Final Exam (2007)	Final Exam [corrected] (2007 - not available)
Final Exam (2006)	Final Exam [corrected] (2006 - not available)
Final Exam (2005)	Final Exam [corrected] (2005 - not available)
Final Exam (2004)	Final Exam [corrected] (2004 - not available)